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Effects of niobium-loading on sulfur dioxide gas-sensing characteristics of hydrothermally prepared tungsten oxide thick film
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Document Title
Effects of niobium-loading on sulfur dioxide gas-sensing characteristics of hydrothermally prepared tungsten oxide thick film
Author
Kruefu V., Wisitsoraat A., Phanichphant S.
Name from Authors Collection
Affiliations
Program in Materials Science, Faculty of Science, Maejo University, Chiang Mai, 50290, Thailand; National Electronics and Computer Technology Center, National Science and Technology Development Agency, Pathum Thani, 12120, Thailand; Materials Science Research Center, Faculty of Science, Chiang Mai University, Chiang Mai, 50200, Thailand
Type
Article
Source Title
Journal of Nanomaterials
ISSN
16874110
Year
2015
Volume
2015
Open Access
Gold, Green
Publisher
Hindawi Publishing Corporation
DOI
10.1155/2015/820509
Abstract
Nb-loaded hexagonal WO3 nanorods with 0-1.0 wt% loading levels were successfully synthesized by a simple hydrothermal and impregnation process and characterized for SO2 sensing. Nb-loaded WO3 sensing films were produced by spin coating on alumina substrate with interdigitated gold electrodes and annealed at 450°C for 3 h in air. Structural characterization by X-ray diffraction, high-resolution transmission electron microscopy, and Brunauer-Emmett-Teller analysis showed that spherical, oval, and rod-like Nb nanoparticles with 5-15 nm mean diameter were uniformly dispersed on hexagonal WO3 nanorods with 50-250 nm diameter and 100 nm-5 μm length. It was found that the optimal Nb loading level of 0.5 wt% provides substantial enhancement of SO2 response but the response became deteriorated at lower and higher loading levels. The 0.50 wt% Nb-loaded WO3 nanorod sensing film exhibits the best SO2 sensing performances with a high sensor response of 10 and a short response time of 6 seconds to 500 ppm of SO2 at a relatively low optimal operating temperature of 250°C. Therefore, Nb loading is an effective mean to improve the SO2 gas-sensing performances of hydrothermally prepared WO3 nanorods. © 2015 Viruntachar Kruefu et al.
Industrial Classification
Knowledge Taxonomy Level 1
Knowledge Taxonomy Level 2
Knowledge Taxonomy Level 3
License
CC BY
Rights
Author
Publication Source
Scopus